5-nitroisophthalic acid
Basic Information:
Nhanganyaya: 5-nitroisophthalic acid chinhu chakakosha chepakati chevasiri-ionic kusiyanisa maajenti senge iodohexyl doro, iodoparol, iodoformol, zvichingodaro. Ndiwo zvakare mavambo ekuparadzira dhayi 2, 6-dicyano-4-nitroaniline, ine zvakasiyana-siyana zvekushandisa uye tarisiro yemusika.
Zita remakemikari: 5-nitroisophthalic acid;5-nitro-1, 3-phthalic acid
Nhamba yeCAS: 618-88-2
Molecular formula: C8H5NO6
Molecular uremu: 211.13
EINECS nhamba: 210-568-3
Mamiriro ezvinhu:
Zvikamu zvinoenderana: Organic makemikari mbishi zvinhu;Pharmaceutical intermediates;
Nzvimbo yekunyungudika: 259-261 °C (lit.)
Poindi yekubikira: 350.79°C (yakaomarara fungidziro)
Density: 1.6342 (yakashata fungidziro)
Refractive index: 1.5282 (kufungidzira)
Painopenya: 120°C
Solubility: Soluble mudoro, ether uye mvura inopisa
zvinhu: chena kusvika kuchena poda.
Mutsipa wehutsi: 0.0±1.2 mmHg pa25°C
| tsanangudzo | unit | standard |
| Chitarisiko | Muchena kusvika kuhupfu huchena | |
| Content | % | ≥99% |
| Unyoro | % | ≤0.5 |
Chinhu chakakosha chepakati chekuparadzira dhayi.Iyo zvakare yepakati peiyo yekuongorora mushonga mutsva ubiquitin (X-ray musiyano mumiririri);Inoshandiswawo kugadzira riwaya remushonga wemushonga wakavakirwa paPDE IV inhibitor glycolinic acid;Inoshandiswawo seyepakati yekuparadzira dhayi (blue azo dyes).
Yakaiswa sulfuric acid (104.3mL, 1.92mol) yakawedzerwa mumabhodhoro matatu, ipapo isophthalic acid (40g, 0.24mol) yakawedzerwa, yakamutswa uye inopisa kusvika 60 ℃, yakachengetwa kwe0.5h, uye 60% nitric acid (37.8g, 0.36) mol) yakawedzerwa kudzora dhigirii rekumhanyisa kudonha.Wedzera mumaawa maviri.Mushure mekuwedzera, kupisa kwekuchengetedza maitiro pa60 ℃ kwemaawa maviri.Kutonhora kusvika pasi pe50 ° C, wobva wawedzera 100mL yemvura.Nyaya yacho yakanyoroveswa kusvika kune tembiricha yekamuri, yakadururirwa musefa, yakapombwa kuti ibvise marara asidhi, keke resefa yakashambidzwa nemvura, yakanyungudutswa kuti iite recrystallize, uye chigadzirwa chichena chaive 34.6 gramu, goho raive 68,4%.
25kg/ 3-in-1 bepa-purasitiki rinoumbwa bhegi, kana bhegi rakarukwa, kana 25kg/ makadhibhokisi bhaketi (φ410 × 480mm);Packaging maererano nezvinodiwa nevatengi;
Chengetedza mumudziyo usingapindi mhepo munzvimbo inotonhorera, yakaoma, inofefetera zvakanaka kure nemoto uye zvinobvira.
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